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Not all contact-angle measurements are created equal: the right method depends on the application. A sessile drop and a tilted plate can give very different, and equally correct, numbers.
Check how well paper and board resist water by reading the water contact angle over time, the measurement ISO/TS 14778 describes. The Dropometer reads the angle at fixed times from about 0.1 s, with ±0.35° accuracy (Dropometer product specification), on a drop shape method validated in two peer reviewed papers. It is too slow for the method's first reading at 20 to 40 ms.
What brings you here?
Quality manager
You need a water check that gives a number, not a judgement call. Angles at fixed times give you values per grade that you can trend by reel and by shift.
Process engineer
You need to see how a change in sizing or coating shifts water resistance. Read every grade at the same times and set limits from your own runs.
R&D
You need to know whether you need the first 40 ms, later readings or grams of water absorbed. Use the decision tree to pick the method.
Free one page checklist for ISO/TS 14778: what to prepare, the reading times to lock, what the Dropometer can and cannot capture, and what to record. Made for paper and board QC benches.
Talk to an expert
Tell us your grade, sizing and current water test. We will show the measurement live and tell you plainly which ISO/TS 14778 readings the Dropometer can take and which need a high speed tester.
ISO/TS 14778:2021, Paper and board: Measurement of water contact angle by optical methods, a Technical Specification from ISO/TC 6/SC 2. ISO confirmed it at the 2024 systematic review. See the ISO listing.
Partially compliant. The method calls for image capture at 50 frames per second or faster and a first reading within 20 to 40 ms of contact. The Dropometer captures at 10 frames per second, so it covers fixed time readings from about 0.1 s only.
Contact angle range 10° to 175°, accuracy ±0.35°, display resolution 0.01°, camera 10 frames per second, from the Dropometer product specification.
The drop shape method is validated against a KRUSS DSA100E in two peer reviewed papers. See our validation publications.
A labels and office products manufacturer uses the Dropometer to see how inks and adhesives wet film, paper, board and plastic. Read the case study.
Contact angle does not give grams of water absorbed. For that, use the Cobb test to ISO 535 or TAPPI T 441.
What this standard measures, who uses it and how the Dropometer fits
ISO 14778, published as ISO/TS 14778:2021, measures the water contact angle on paper and board with automated optical equipment: a higher, steadier angle means the sheet resists water better. Paper mills, board converters and packaging labs use it in quality control to check sizing and how fast water wets and soaks into the sheet. The Dropometer is partially compliant: it reads the angle at fixed times from about 0.1 s, but it cannot take the method's first reading at 20 to 40 ms.
The method places a water drop on a flat test piece and measures the droplet shape in contact with the solid as it spreads and soaks in. ISO calls for image capture at 50 frames per second or faster, so the first angle is read before an absorbent sheet takes up the drop (source: ISO/TS 14778:2021 listing). It suits most kinds of paper or board, but not structured materials.
The Dropometer contact angle and surface energy kit captures at 10 frames per second. That suits readings at about 0.1 s, 1 s, 10 s and later, which show how the angle falls as the sheet absorbs water. To keep those readings comparable between operators and sites, follow our steps for reproducible contact angle measurement and the contact angle measurement guide. If you need the full high speed method, our buying guide for ISO and GLP regulated high throughput QC compares the options.
Further reading: the packaging and containers guide, wicking control for paper microfluidic and lateral flow tests, wettability in our glossary, and water contact angle reference values for common surfaces.
The ISO/TS 14778 measurement, step by step, in our own words
These steps outline the procedure and show where the Dropometer fits. They do not replace the standard. Buy the current edition and follow its drop volume, timing, conditioning and specimen rules.
From the Dropometer product specification. Display resolution is 0.01°.
Fine for readings from about 0.1 s on. Too slow for the 20 to 40 ms first reading.
Base plate, phone holder, LED and syringe. No PC needed.
Cut flat test pieces and mark the side you test. Handle them by the edges, because skin oils change the angle. Condition and test them in the atmosphere the standard specifies.
Place the base plate on a level bench, mount the phone and LED, and fill the syringe with water of the grade the standard specifies. Lay the test piece flat on the sessile stage, test side up.
Dispense the drop volume the standard specifies. The automatic dropper add-on helps keep the volume the same for every drop. Do not touch the sheet with the needle.
Capture the drop as it spreads and soaks in, and read the angle at your agreed times, for example about 0.1 s, 1 s and 10 s. At 10 frames per second the first frame can land at any point in the first 0.1 s, so the Dropometer cannot supply the 20 to 40 ms reading.
Place several drops on fresh, unwetted areas of each test piece. Sizing and formation vary across the sheet, so one drop is not enough.
Record the mean and spread at each time, the side tested, grade and room conditions. Compare with limits from your own study. Check your numbers against our water contact angle reference values for a sanity check.
This video shows a complete Dropometer contact angle measurement, from setup to result. It covers the steps above in one run.
Independent benchmarking and publication-based validation references.
Peer reviewed method
The Dropometer drop shape method is validated against a KRUSS DSA100E in two peer reviewed papers, one in Review of Scientific Instruments and one in Colloids and Surfaces A. Published contact angle accuracy is ±0.35°.
Customer evidence
We have no published client paper on ISO/TS 14778 yet. A labels manufacturer uses the Dropometer in two labs to check how inks, adhesives and coatings wet paper, board and film.
ISO/TS 14778 · sizing · paper and board QC
The public ISO/TS 14778 summary gives no pass or fail angle for paper or board (source: ISO/TS 14778:2021 listing). Limits are set from your own correlation or capability study.
Measure grades that printed, glued and held up to water well, and grades that failed. Read each one at the same fixed times, for example about 0.1 s, 1 s and 10 s. Then set an accept limit on the angle at one time, or on how far it falls between two times.
If your limit depends on the angle in the first 40 ms, the Dropometer cannot supply it. Use a tester that captures at 50 frames per second or faster for that reading. Repeat the study when you change furnish, sizing agent, coating or calender settings.
Example data for illustration only. These are not measured results. Your own grades, sizing and limits decide the numbers.
| Grade | Drops (n) | About 0.1 s (°) | 1 s (°) | 10 s (°) | Reading |
|---|---|---|---|---|---|
| Coated board, print side | 10 | 98.4 | 97.1 | 94.6 | Stable angle: strong water resistance |
| Hard sized liner | 10 | 92.3 | 86.0 | 74.5 | Slow fall: compare with your limit |
| Lightly sized paper | 10 | 78.6 | 55.2 | 22.4 | Fast fall: review sizing |
| Unsized tissue | 10 | Below 10° | Below 10° | Below 10° | Soaked in before 0.1 s: needs a high speed tester |
Each value is the mean of ten drops on one grade. Readings at about 0.1 s, 1 s and 10 s are later fixed times the Dropometer can capture. No published limits apply: the reading column shows how an example lab might act after its own correlation study.
The same example data as the table, plotted on a log time axis. The unsized tissue is left out because its drop soaked in before the first reading.
Example data, not measured results.
What changes when the water check is a measured angle over time
| Metric | Before Dropometer | With Dropometer | Results |
|---|---|---|---|
| How the check is made | Water drop or feather test, judged by eye | Water contact angle read from the drop image at fixed times | No published benchmark |
| Result format | Pass or fail, or soak time by stopwatch | An angle per drop per time, 0.01° display, ±0.35° accuracy | Dropometer product specification |
| Earliest reading | High speed tester: within 20 to 40 ms of contact | Dropometer: about 0.1 s, at 10 frames per second | ISO/TS 14778:2021 listing; Dropometer product specification |
| Where it runs | Shared lab tester | At the machine or in the lab, on battery for up to 8 h | Dropometer product specification |
Bring two samples: one grade that held up to water and one that did not. We will measure both live and show the angle at each reading time.
Enter your own numbers. The defaults are examples, not Droplet Lab results.
Quality cost snapshot
Result
Annual exposure combines audit/CAPA cost, customer rejections, and recall probability; avoided exposure applies the risk reduction percentage.
Lock these before you compare results between shifts or sites
| Parameter | Recommended Setting | Technical Rationale |
|---|---|---|
| Test liquid | Water of the grade the standard specifies | This is a water contact angle method. Other liquids belong to other methods. |
| Drop type | Sessile drop, angle read over time | Paper and board absorb water, so the angle falls after contact. |
| Drop volume | As the standard specifies, fixed for every drop | A changing volume changes how fast the drop soaks in. |
| First reading | Within 20 to 40 ms, at 50 frames per second or faster | ISO/TS 14778 scope. The Dropometer captures at 10 frames per second and cannot take this reading. |
| Later readings | Fixed times you agree, for example about 0.1 s, 1 s and 10 s | The Dropometer covers these. Keep the same times for every drop and grade. |
| Fit model | Young-Laplace or polynomial, the same for every run | Both models are in the Dropometer software. Do not mix them within one study. |
| Replicates | Several drops on fresh areas of each test piece | Sizing and formation vary across the sheet. |
| Environment | Condition and test as the standard specifies; record temperature and humidity | Paper picks up moisture from the air. The Dropometer runs at 10 to 45 °C and has no humidity control. |
Pick the method by the question you need answered
Start: What do you need to know about water on your paper or board?
Your sheet absorbs water fast, or your customer names ISO/TS 14778 and its first reading.
Use ISO/TS 14778 on a tester that captures at 50 frames per second or faster. The Dropometer cannot take this reading.
You want to trend sizing by how the angle falls at about 0.1 s, 1 s and 10 s.
The Dropometer takes these readings: partially compliant with ISO/TS 14778. For automated checkpoints at the same times, see TAPPI T 558.
Your specification names the older TAPPI method for writing and ruling quality.
Use TAPPI T 458 / ASTM D724. The Dropometer covers those reading times.
You need water absorptiveness in g/m² over a set time, not an angle.
Use the Cobb test to ISO 535 or TAPPI T 441. Contact angle complements it.
Start from the question you need answered. Blue boxes are measurements the Dropometer runs.
Is ISO/TS 14778 the right test?
What the angle over time tells you, and what it does not
Honest limits of the method and of the Dropometer
No. It is ISO/TS 14778:2021, a Technical Specification and the first edition. ISO reviewed and confirmed it in 2024, so it is still current. Quote the full designation, ISO/TS 14778:2021, in your test report.
Partly. ISO/TS 14778 calls for capture at 50 frames per second or faster and a first reading within 20 to 40 ms of contact. The Dropometer captures at 10 frames per second. It reads the angle at fixed times from about 0.1 s with ±0.35° accuracy, but not that first reading.
Absorbent paper can take up a water drop within a fraction of a second. A fast camera reads the angle before the drop soaks in. On sized or coated grades the angle falls slowly, so later readings still tell you a lot.
TAPPI T 458 is an older classical method that reads the angle at 5 s and 60 s (TAPPI T 458 review draft, 2024). TAPPI T 558 uses an automated tester with checkpoints at 0.1 s, 1 s and 10 s (TAPPI T 558 review draft, 2025). ISO/TS 14778 also uses automated capture and adds the 20 to 40 ms first reading. See TAPPI T 458 and TAPPI T 558.
The public summary of ISO/TS 14778 gives no pass or fail angle. Set limits from your own correlation study: measure grades that held up to water and grades that failed, at the same reading times.
No. The Cobb test gives grams of water absorbed per square metre in a set time. Contact angle shows how water wets the surface and how fast that changes. Many mills run both. See ISO 535 and TAPPI T 441.
This page summarises ISO/TS 14778:2021 in our own words and does not reproduce the standard. Buy the current edition from ISO or your national standards body before you write a procedure. Droplet Lab does not certify compliance. Your own method validation does.
Sources, review and tools
ISO/TS 14778:2021 listing; BSI PD ISO/TS 14778:2021 listing; iTeh ISO/TS 14778:2021 preview (scope and contents); TAPPI T 558 review draft, 2025, the Dropometer product specification and Droplet Lab validation papers.
Drafted with Claude (Anthropic) from the sources listed, then reviewed by Droplet Lab.
We did not copy text from the standard. Buy the current edition for the full procedure.
October 2026
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